Marian Vasilescu July 3, 2020

Microscopy lab company in Chelmsford, MA? The diameter, perimeter, shape and aggregation patterning of particles are often of interest with manufactured or naturally occurring materials. Our PSA method is useful to measure and document the morphology and distribution of a sample. Whether you have particles, pores or film coatings, we can accommodate your project needs. Scanning Electron Microscopy (SEM)

Approach: MicroVision Labs’ staff consulted with the client, and determined that, unfortunately, there could be a number of potential sources of a white material. Even before the bottle with the suspended material arrived, it was determined that there was less than 50 mL of water remaining, and likely less than a gram of material suspended in the water. The client was aware that this material could represent precipitated minerals from the source water, a polymer residue from the bottles, some form of biological tissue that might have formed despite sterilization procedures, or could very well represent some completely unforeseen foreign material. The issue facing the client is how to have the material tested, as most tests that they might request for one or the other of these known potential sources would destroy or alter the sample. Choosing a test was therefore something of a gamble, because if they tested for calcium (mineral precipitate) and it came up negative – that didn’t actually tell them what the powder was, just that it didn’t have any calcium. Based on this conversation, the non-destructive, specialized testing at MicroVision Laboratories was chosen as the best choice.

The profile of the flow of the solder at these bonds was documented using the SEM with backscatter imaging, which correlates brightness in the image with atomic density. Some voids were found in the solder as shown the SEM image. An EDS spectrum of the solder was acquired which showed that the solder was a tin/lead (80/20) solder. The EDS map clearly shows the copper wire and copper pad (red) with the tin lead solder (light blue) that appears to have flowed well and made a good bond between the copper elements. This map also shows the fiberglass bundles that add structural integrity to the board.

Do you do any animal testing? No. Do you analyze any tissue samples or blood samples? No. We do not do any blood analyses and we are not set up to prepare tissue samples. What are some of the cool samples you have looked at under the scanning electron microscope? We have seen 10,000 year old Wolly Mammoth hair, meteorites, an artificial heart valve, civil war bullets, insulin pumps, rare colonial coins, a kidney stone, and a few things we can’t talk about. But some of the more mundane samples, like wood or salt crystals, have proven to be extremely interesting subjects to image. Explore even more info on https://microvisionlabs.com/imaging-technology/.

The data indicated that a significant portion of the dust was from the insulation in the attic. The contractor had replaced a portion of duct work running to the master bedroom. During this replacement, fiberglass insulation was knocked into the ducting. The small glass insulation fibers were spread through the AC ducts and settling out of the air throughout the house. The client was relieved to know what was causing their skin irritation and the significant dust build up. Using the results garnered from the analysis from MicroVision Labs they were able to have the contractor clean out the duct work and act to prevent further spread of the insulation fibers and properly clean up the settled dust in the house that was the cause of the homeowner’s skin irritation.

?We partner with companies in all phases of product development and sales, including R&D, manufacturing, QC, advertising and failure analysis. Our laboratory offers a highly-trained and experienced staff utilizing a powerful set of analytical tools (SEM with EDS and backscatter detectors, Bruker X-Flash elemental mapping, X-Ray imaging, Micro-FTIR spectroscopy, Micro-XRF, light microscopy, cross sectioning/precision polishing and microhardness testing). See extra details at https://microvisionlabs.com/.